凈化裝置/藥典/二氧化碳/CO2
凈化裝置/藥典/二氧化碳/CO2 詳細(xì)信息:
型號(hào):HHO-III Purification
應(yīng)用:藥典二氧化碳中碳?xì)浠衔餃y(cè)定
2015版藥典四部二氧化碳中碳?xì)浠衔镯?xiàng)方法描述如下:“取本品作為供試品;取甲烷含量為0.0020%的氣體(以氮?dú)鉃橄♂寗┳鳛閷?duì)照氣體,照氣相色譜法(通則0521)試驗(yàn),用玻璃球?yàn)樘盍系纳V柱(0.8mX4mm,8 0目);柱溫為110°C;進(jìn)樣口溫度為110°C ; 檢測(cè)器溫度為120°C。量取供試品氣體與對(duì)照氣體,注入氣相色譜儀,在凈化溫度為360°C時(shí)測(cè)得的峰面積為相應(yīng)空白值;量取供試品氣體與對(duì)照氣體,注人氣相色譜儀,測(cè)定峰面積,減去相應(yīng)空白值后的峰面積為校正峰面積。按外標(biāo)法以校正峰面積計(jì)算,含碳?xì)浠衔铮ㄒ约淄橛?jì))不得過(guò)0.0020%。"
這其中凈化溫度具體是指什么?是否因?yàn)樗幍浞椒枋霾粔蛟敱M,實(shí)際是甲烷轉(zhuǎn)化器之類的轉(zhuǎn)化溫度?
許多制藥企業(yè)很困惑,以為凈化溫度就是甲烷轉(zhuǎn)化爐,其實(shí)這是不對(duì)的。
凈化裝置/藥典/二氧化碳/CO2 圖片:
Purification device / pharmacopoeia / carbon dioxide / CO2
Purification unit / Pharmacopoeia / CO2 / CO2 Details:
Model: HHO-III Purification
Application: Determination of hydrocarbons in carbon dioxide in Chinese Pharmacopoeia
The 2015 version of the Pharmacopoeia four carbon dioxide hydrocarbons method is described as follows: "take this product as a test sample; take a gas with a methane content of 0.0020% (with nitrogen as a diluent) as a control gas, by gas chromatography (General Rule 0521) Test, using a glass ball as a packing column (0.8mX4mm, 80 mesh); column temperature is 110 ° C; inlet temperature is 110 ° C; detector temperature is 120 ° C. Measure the gas and test The control gas is injected into the gas chromatograph, and the peak area measured at the purification temperature of 360 ° C is the corresponding blank value; the gas for the test sample and the control gas are taken, and the gas chromatograph is injected to determine the peak area, and the corresponding blank is subtracted. The peak area after the value is the corrected peak area. The hydrocarbon-containing compound (in terms of methane) shall not exceed 0.0020% by the external standard method.
What does the purification temperature mean? Is it because the Pharmacopoeia method description is not detailed enough, is it actually a conversion temperature such as a methanator?
Many pharmaceutical companies are confused, thinking that the purification temperature is a methane reformer. In fact, this is a big mistake.
Tengzhou Haohao Chromatography Instrument Technology Service Co., Ltd., relying on the R&D center of Hong Kong, China, successfully developed a purification device, which is original in China and is currently applying for patent protection.
Purification unit / Pharmacopoeia / CO2 / CO2 Picture: