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浩瀚色譜(山東)應(yīng)用技術(shù)開發(fā)有限公司


當(dāng)前位置:浩瀚色譜(山東)應(yīng)用技術(shù)開發(fā)有限公司>>>>毛細(xì)管柱測定CO2中碳?xì)浠衔?

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毛細(xì)管柱測定CO2中碳?xì)浠衔?,非甲烷總烴,液化石油氣,頂空進樣器,粗苯,三苯,環(huán)氧乙烷,三甲胺,二甲醚,植物油,脂肪酸甲酯

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毛細(xì)管柱測定CO2中碳?xì)浠衔?/strong>
毛細(xì)管柱測定CO2中碳?xì)浠衔?/strong> 詳細(xì)信息:

規(guī)格:30m*0.53mm

型號:HH-THC-30

應(yīng)用:藥典二氧化碳中碳?xì)浠衔餃y定


2015版藥典四部二氧化碳中碳?xì)浠衔镯椃椒枋鋈缦拢骸叭”酒纷鳛楣┰嚻?;取甲烷含量?.0020%的氣體(以氮氣為稀釋劑)作為對照氣體,照氣相色譜法(通則0521)試驗,用玻璃球為填料的色譜柱(0.8mX4mm,8 0目);柱溫為110°C;進樣口溫度為110°C ; 檢測器溫度為120°C。量取供試品氣體與對照氣體,注入氣相色譜儀,在凈化溫度為360°C時測得的峰面積為相應(yīng)空白值;量取供試品氣體與對照氣體,注人氣相色譜儀,測定峰面積,減去相應(yīng)空白值后的峰面積為校正峰面積。按外標(biāo)法以校正峰面積計算,含碳?xì)浠衔铮ㄒ约淄橛?不得過0.0020%。"

隨著氣相色譜儀的發(fā)展,許多制藥企業(yè)購置的是毛細(xì)管進口系統(tǒng)的氣相色譜,因此填充柱接不上,需要改造儀器,十分麻煩,滕州市浩瀚色譜儀器技術(shù)服務(wù)有限公司,與時俱進,研發(fā)毛細(xì)管柱測定CO2中碳?xì)浠衔?/strong>,安裝方便,儀器無需改造,效率高,結(jié)果滿意。







Determination of Hydrocarbons in CO2 by Capillary Column
Determination of Hydrocarbons in CO2 by Capillary Columns

Specification: 30m*0.53mm
Model: HH-THC-30
Application: Determination of hydrocarbons in carbon dioxide in Chinese Pharmacopoeia

The 2015 version of the Pharmacopoeia four carbon dioxide hydrocarbons method is described as follows: "take this product as a test sample; take a gas with a methane content of 0.0020% (with nitrogen as a diluent) as a control gas, by gas chromatography (General Rule 0521) Test, using a glass ball as a packing column (0.8mX4mm, 80 mesh); column temperature is 110 ° C; inlet temperature is 110 ° C; detector temperature is 120 ° C. Measure the gas and test The control gas is injected into the gas chromatograph, and the peak area measured at the purification temperature of 360 ° C is the corresponding blank value; the gas for the test sample and the control gas are taken, and the gas chromatograph is injected to determine the peak area, and the corresponding blank is subtracted. The peak area after the value is the corrected peak area. The hydrocarbon-containing compound (in terms of methane) shall not exceed 0.0020% by the external standard method.
With the development of gas chromatographs, many pharmaceutical companies purchase gas chromatography of capillary inlet systems, so the filling column can not be connected, and it is very troublesome to modify the instrument. Tengzhou Haohao Chromatography Instrument Technology Service Co., Ltd. keeps pace with the times. The development of capillary column for the determination of hydrocarbons in CO2 is easy to install, the instrument does not need to be modified, the efficiency is high, and the results are satisfactory.

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